did i ruin it ?

i wound up just puting all reta i have in freezer since i didnt know how long it will take me to use it. when im ready for next one i just put in fridge to defrost it then the day i add the bac i let it sit on table for a little. i took 8 mg but i barely feel it, did puting it in freezer ruin it? im also on 200 mg week test so im not sure if im just getting appetite from that plus water weight